(This was Chem 545, 542, 625 in previous years.)
NMR is arguably the most powerful analytical tool in modern chemical research. It encompasses a broad spectrum of techniques and information- from counting the number of protons in a molecule to determining 3-D structures and distances.
This class in intended to provide NMR training to all students (both undergraduate and graduate) who expect to use the NMR facility in their research. The class consists of lectures once a week, and individual instrument training. Typically, students require about 20 training sessions to complete training on basic experiments on all three spectrometers.
There is no prerequisite, but 1 semester of physical chemistry is suggested.
All classes will be held via Zoom from 1:00- 2:50 pm on Fridays.
22 Jan
no class
29 Jan
class overview
NMR Theory
5 Feb
Data Acquisition
Instrumental parameters
Instrumental design
Locking and Shimming
12 Feb
Data Processing
Processing Parameters
Apodizations
Data "Corrections
Solution Experiments
"Simple 1D"
Decoupling
NOE
Relaxation (T1 and T2)
DEPT
19 Feb
Multi-dimensional experiments
COSY (Correlated spectroscopy)
NOESY (NOE spectroscopy)
Hetcorr/HMQC
26 Feb
Introduction to Solid-State NMR
Theory
MASS/VASS/DOR
CP
CSA
2D solids
5 Mar
Advanced Topics
Hints, Problems
Review
12 Mar
Introduction to Mass Spectrometery
guest lecture by Dr. Bani Ghosh,
Director, CCB Mass Spec Facility
19 Mar
No class UNM spring break
26 Mar
Final during class time
2 Apr
No class unless schedule slips
For more information, contact
Karen Ann Smith, Director NMR Facility, University of New Mexico Department of Chemistry Clark Hall Albuquerque, NM 87131-1096 karenann@unm.edu 505-277-4031 voice, 505-277-2609 fax